Acta Chimica Sinica ›› 1959, Vol. 25 ›› Issue (6): 420-423. Previous Articles     Next Articles

用气液色谱法分离甲基氯硅烷和鉴定的研究

余仲建1,2, 杨学谨1,2, 粟富经1,2, 谢珍珍1,2, 刘静华1,2   

  1. 1. 中国科学院河北分院元素有机研究所;
    2. 南开大学化学系
  • 收稿日期:1959-07-30 出版日期:1959-12-15 发布日期:2013-06-03

GAS-LIQUID CHROMATOGRAPHIC SEPARATION AND IDENTIFICATION OF METHYLCHLOROSILANES

YU CHUNG-CHIEN1,2, YANG HSÜEH-CHING1,2, SU FU-CHING1,2, HSIEH CHEN-CHEN1,2, LIU CHING-HUA1,2   

  1. Department of Chemistry, Nankai University
  • Received:1959-07-30 Online:1959-12-15 Published:2013-06-03

Benzophenone has been found to be a suitable fixed phase for gas-liquid chromato-graphy of methylchlorosilanes.Good separation of methyltrichlorosilane, dimethyldichlorusi-lane, trimethylchlorosilane and silicon tetrachloride was obtained at 52℃.