Chin. J. Org. Chem. ›› 2008, Vol. 28 ›› Issue (09): 1641-1645. Previous Articles     Next Articles



王道林*; 韩 珊; 谷 峥 ; 徐 姣   

  1. (渤海大学化学化工学院 辽宁省应用化学重点实验室 锦州 121003)
  • 收稿日期:2007-12-26 修回日期:2008-03-27 发布日期:2008-09-20
  • 通讯作者: 王道林

Synthesis of 1-(2-Benzo[b]furoyl)guaiazulene Derivatives

WANG, Dao-Lin*; HAN, Shan; GU, Zheng; XU, Jiao   

  1. (Liaoning Key Laboratory of Applied Chemistry, College of Chemistry and Chemical Engineering,
    Bohai University, Jinzhou 121003)
  • Received:2007-12-26 Revised:2008-03-27 Published:2008-09-20
  • Contact: WANG, Dao-Lin

1-(2-Benzo[b]furoyl)guaiazulene derivatives were synthesized by the condensation of 3-(chloroacetyl)guaiazulene with salicylaldehydes under mild conditions with good yields. The chloroacety-lation conditions of guaiazulene with chloroacetyl chloride were discussed. All the compounds were fully characterized by 1H NMR, IR spectra and elemental analysis.

Key words: azulene, chloroacetylation, salicylaldehyde, synthesis, guaiazulene, benzo[b]furan