Chin. J. Org. Chem. ›› 2008, Vol. 28 ›› Issue (10): 1813-1815. Previous Articles     Next Articles



刘天宝*,a ; 彭艳芬a ; 邹建平b   

  1. (a池州学院化学与食品科学系 池州 247000)
    (b苏州大学化学化工学院 苏州 215123)
  • 收稿日期:2007-11-11 修回日期:2008-04-25 发布日期:2008-10-20
  • 通讯作者: 刘天宝

Synthesis of 1-Phenyl-5-aryl-1,2-dihydro-1,2,4-triazole-3-thione Derivatives

LIU, Tian-Bao*,a ; PENG, Yan-Fen a; ZOU, Jian-Pingb   

  1. (a Department of Chemistry and Food Science, Chizhou College, Chizhou 247000)
    (b Department of Chemistry, Suzhou University, Suzhou 215123)
  • Received:2007-11-11 Revised:2008-04-25 Published:2008-10-20
  • Contact: LIU, Tian-Bao

Substituted benzoyl chlorides were reacted with potassium isothiocyanate, and the resulting intermediates were then reacted with phenyl hydrazine to give the title compounds 1-phenyl-5- aryl-1,2-dihydro-1,2,4-triazole-3-thione derivatives. Their structures were characterized by IR, 1H NMR, 13C NMR and HRMS data.

Key words: substituted benzoyl chloride, 1,2,4-triazole-3(2H)-thione, phenylhydrazine