Chinese Journal of Organic Chemistry 2010, 30(05) 745-748 DOI:     ISSN: 0253-2786 CN: 31-1321/O6
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Keywords
cyanuric chloride
cyclophane
synthesis
characterization
Authors
吕Guo-Hua
HUA Cheng-Wen
GOU Xiao-Feng
LIU Yan-Feng
PubMed
Article by 吕G. H.
Article by Hua, C. W.
Article by Gou, X. F.
Article by Liu, Y. F.

Synthesis and Characterization of Azacyclophanes Containing 1,3,5-Triazine

Lü Guo-Hua , HUA Cheng-Wen, GOU Xiao-Feng, LIU Yan-Feng

(Key Laboratory of Synthetic and Natural Functional Molecule Chemistry, Ministry of Education, College of Chemistry & Materials Science, Northwest University, Xi an 710069)

Abstract：

Cyclophane with a cavity structure, has a great potential prospects. Some novel azacyclophanes were synthesized from cyanuric chloride, phenol, sodium methoxide, 1,6-hexane diamine and 4,4 -diaminodiphenyl methane by substitution, and their structures were characterized by 1H NMR, IR, MALDI-TOF-MS techniques and elemental analysis. A large number of experiments have been carried out to explore the solvent, alkal and concentration to find out the best reaction conditions.

Keywords： cyanuric chloride   cyclophane   synthesis   characterization  
Received 2009-09-08 Revised 2009-11-25 Online: 2009-12-17 
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Email: huachengwen@126.com
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