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Chinese Journal of Chemistry 2009, 27(10) 1989-1994 DOI:
ISSN: 1001-604X CN: 31-1547/O6 |
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An Efficient Synthesis of 4H-Benzo[g]chromene-5,10-dione De- rivatives through Triethylbenzylammonium Chloride Catalyzed Multicomponent Reaction under Solvent-free Conditions |
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YAO Changsheng 1,2; YU Chenxia 1,2; LI Tuanjie 1,2; TU Shujiang *,1,2 |
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a School of Chemistry & Chemical Engineering, Xuzhou Normal University, Xuzhou, Jiangsu 221116, China
b Key Laboratory of Biotechnology for Medicinal Plants, Xuzhou Normal University, Xuzhou, Jiangsu 221116, China |
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Abstract：
A series of 4-aryl-5,10-dihydro-4H-benzo[g]chromene-5,10-dione derivatives were synthesized by a three-component reaction with aromatic aldehyde, 2-hydroxy-1,4-dihydronaphthalene-1,4-dione, and malononitrile catalyzed by triethylbenzylammonium chloride under solvent-free conditions. The novel efficient method has the advantages of environmental friendliness, high yield, simple work-up and ease of operation. |
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Keywords：
4-aryl-4H-benzo[g]chromene-5
10-dione
solvent-free
three-component reaction
triethylbenzylammonium chloride
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Received 2009-03-11 Revised 2009-04-24 Online: 2009-06-10 |
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Email: laotu2001@263.net |
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