Acta Chimica Sinica ›› 1963, Vol. 29 ›› Issue (4): 291-294. Previous Articles     Next Articles

有机磷胺化合物之研究——Ⅲ.通法制备烴氧基烴基膦酰胺及二烴氧基硫磷酰胺

童曾寿   

  1. 北京医学科学院
  • 收稿日期:1962-08-06 出版日期:1963-08-15 发布日期:2013-06-03

STUDIES ON THE ORGANIC AMIDO-PHOSPHORUS COMPOUNDS——Ⅲ. SYNTHESIS OF O-ALKYL ALKYLPHOSPHONAMIDES AND O, O’-DIALKYL THIOPHOSPHORAMIDES

TUNG TZENG-SHOU   

  1. Peking Institute of Medical Sciences
  • Received:1962-08-06 Online:1963-08-15 Published:2013-06-03

A general method for the synthesis of O-alkyl alkylphosphonamides and O,O-dialkyl thiophosphoramides has been reported.This method is based on the reactions of esters of alkylphosphonous acid and dialkyl thiophosphites with amines in the presence of carbon tetrachloride.The reaction mechanism is discussed.