Synthesis of 3-(2'-phenyl-1', 2', 3'-triazole-4'-yl)-6-alkyl/aryl-s-triazolo[3, 4-b]-1, 3, 4-thiadiazoles

Acta Chimica Sinica ›› 1998, Vol. 56 ›› Issue (6): 618-624. Previous Articles

Original Articles

3-(2'-苯基-1', 2', 3'-连三唑-4'-基)-6-烷基/芳基-均三唑并[3, 4-b]-1, 3, 4-噻二唑的合成

刘方明;于建新;刘育亭;陈耀祖

新疆大学化学系;浙江大学化学系

发布日期:1998-06-15

Synthesis of 3-(2'-phenyl-1', 2', 3'-triazole-4'-yl)-6-alkyl/aryl-s-triazolo[3, 4-b]-1, 3, 4-thiadiazoles

LIU FANGMING;YU JIANXIN;LIU YUTING;CHEN YAOZU

Published:1998-06-15

Abstract

Condensation of 3-(2'-phenyl-1', 2', 3'-triazole-4'-yl)-4-amino-5-mercapto-1, 2, 4-triazole(1) with alkyl or aryl acids (2a-r) in the presence of phosphorus oxychloride gave 18 novel 3-(2'-phenyl-1', 2', 3'-triazole-4'-yl)-6-alkyl/aryl-s-triazolo[3, 4-b]-1, 3, 4-thiadiazoles (3a-r). Their structures were confirmed by elemental and spectral analyses.

Key words: BIOLOGICAL ACTIVITY, INFRARED SPECTROPHOTOMETRY, ELEMENTAL ANALYSIS, MASS SPECTROGRAPHY, PROTON MAGNETIC RESONANCE SPECTROMETRY, THIADIAZOLE P, PYRRODIAZOLE P

CLC Number:

O621

Cite this article

LIU FANGMING;YU JIANXIN;LIU YUTING;CHEN YAOZU. Synthesis of 3-(2'-phenyl-1', 2', 3'-triazole-4'-yl)-6-alkyl/aryl-s-triazolo[3, 4-b]-1, 3, 4-thiadiazoles[J]. Acta Chimica Sinica, 1998, 56(6): 618-624.

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3-(2'-苯基-1', 2', 3'-连三唑-4'-基)-6-烷基/芳基-均三唑并[3, 4-b]-1, 3, 4-噻二唑的合成

Synthesis of 3-(2'-phenyl-1', 2', 3'-triazole-4'-yl)-6-alkyl/aryl-s-triazolo[3, 4-b]-1, 3, 4-thiadiazoles

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