Flash Evaporation-Gas Chromatography Determination with Pattern Recognition Analysis for Curcuma zedoaria Rosc.

doi:10.6023/A1105164

Acta Chimica Sinica ›› 2012, Vol. 70 ›› Issue (01): 78-82.DOI: 10.6023/A1105164 Previous Articles Next Articles

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莪术药材的闪蒸气相色谱测定及其模式识别分析研究

刘会君^a, 陈爽^b, 王鹏^a, 陆璐^a, 潘再法^a, 王丽丽^a

a. 浙江工业大学化学工程与材料学院, 杭州 310014;
b. 浙江省食品药品检验所, 杭州 310004

投稿日期:2011-06-16 修回日期:2011-09-09 发布日期:2012-02-25
通讯作者: 王丽丽 E-mail:lili_wang@zjut.edu.cn
基金资助:
浙江省重点科技创新团队(No.2011R09002-11)和浙江省重中之重开放基金(No.200908)资助项目.

Flash Evaporation-Gas Chromatography Determination with Pattern Recognition Analysis for Curcuma zedoaria Rosc.

Liu Huijun^a, Chen Shuang^b, Wang Peng^a, Lu Lu^a, Pan Zaifa^a, Wang Lili^a

a. College of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310014;
b. Zhejiang Institute for Food and Drug Control, Hangzhou 310004

Received:2011-06-16 Revised:2011-09-09 Published:2012-02-25
Supported by:
Project was supported by the Key Science and Technology Innovation Team of Zhejiang Province(No.2011R09002-11)and the Opening Foundation of Zhejiang Provincial Top Key Discipline(No.200908).

A method of flash evaporation followed by gas chromatography(FE-GC)was developed for de-termination of volatile components of Curcuma zedoaria Rosc.The Curcuma zedoaria Rosc.samples from 3 different growing places were analyzed on the basis of flash evaporation-gas chromatography(FE-GC).An amount 0.4 mg of sample powder was evaporated in a micro-furnace pyrolyzer at 200℃,and the products formed were introduced into a gas chromatograph equipped with a flame ionization detector or mass spec-trometer.Based on the relative peak areas of 35 peaks in the chromatogram obtained by FE-GC,9 samples of Curcuma zedoaria Rosc.from 3 different origins were clearly classified into 3 categories by two pattern recognition analysis,i.e.principle component analysis and hierarchical cluster analysis.The results proved that it is a simple,rapid and accurate method suitable for quality control of the traditional Chinese medi-cines.

Key words: Curcuma zedoaria Rosc., flash evaporation, gas chromatography, principal component analysis, hierarchical cluster analysis

Cite this article

Liu Huijun, Chen Shuang, Wang Peng, Lu Lu, Pan Zaifa, Wang Lili. Flash Evaporation-Gas Chromatography Determination with Pattern Recognition Analysis for Curcuma zedoaria Rosc.[J]. Acta Chimica Sinica, 2012, 70(01): 78-82.

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莪术药材的闪蒸气相色谱测定及其模式识别分析研究

Flash Evaporation-Gas Chromatography Determination with Pattern Recognition Analysis for Curcuma zedoaria Rosc.

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