Chin. J. Org. Chem. ›› 2003, Vol. 23 ›› Issue (8): 846-849. Previous Articles     Next Articles

室温固相反应一步合成N-亚水杨基-4-氨基安替比林

李人宇;卑凤利;马卫兴;杨绪杰;许兴友;陆路德;汪信   

  1. 南京理工大学材料化学实验室
  • 发布日期:2003-08-25

One Step Sysnthesis of N-Salicylidene-4-aminoantipyrine by Solid Phase Reaction at Room Temperature

Li Renyu;Bei Fengli;Ma Weixing;Yang Xujie;Xu Xingyou;Lu Lude;Wang Xin   

  1. Materials Chemistry Laboratory, Nanjing University of Science and Technology
  • Published:2003-08-25

N-Salicylidene-4-aminoantipyrine was synthesized by the solid phase reaction of 4-aminoantipyrine with salicylaldehyde at room temperature without solvent. The reaction was completed in 15 min in 95% yield. The product was characterized by elemental analysis, IR, *H NMR, X-ray powder diffraction and X-ray single crystal diffraction.

Key words: ANTIPYRINU;SCHIFF BASE;ELEMENTAL ANALYSIS;IR;1HNMR;XRD, STRUCTURE CHARACTERISTICS

CLC Number: