Acta Chimica Sinica ›› 1989, Vol. 47 ›› Issue (8): 804-807. Previous Articles     Next Articles

Original Articles

石墨炉原子吸收光谱中尿的背景吸收研究

莫胜钧   

  1. 华南师范大学化学系
  • 发布日期:1989-08-15

The study of the background absorption of urine sample in the graphite furnace atomic absorption spectroscopy

MO SHENGJUN   

  • Published:1989-08-15

The nature and source of the background absorption of the urine sample and the method of eliminating the background were studied. The wavelength-dependence of urine background is quite similar to that obtained from sodium chloride. This shows that the background absorption of the urine sample arises mainly from sodium chloride. When the general heating mode is used, the outline of the background absorption curves and peak height are dependent on the atomization temperature However, the above dependence is not observed in the case of the max. power heating mode. The background interferences from urine can be decreased by the addition of nitric acid. The choice of appropriate signal recording time, ashing temperature and time, and heating mode are also effective for this purpose.

Key words: ATOMIC ABSORPTION SPECTROPHOTOMETRY, URINE, SODIUM CHLORIDE, GRAPHITIZING FURNACES, AMMONIUM CHLORIDE, HOST IMPROVING AGENTS, ATOMIZATION TEMPERATURE, BACKGROUND ABSORPTION

CLC Number: