Studies on the hydrothermal synthesis of NaZr~2(AsO~4)~3

Abstract

NaZr2(AsO4)3 was synthesized hydrothermally. The effects of the conditions of hydrothermal synthesis on the phases of products were discussed. The process of the hydrothermal crystallization of NaZr2(AsO4)3 was studied. The F-, which was introduced into the hydrothermal synthesis of NaZr2(AsO4)3, lowered the temperature of the crystallization and benefitted the growth of the perfect larger single crystal of NaZr2(AsO4)3. The products obtained in various hydrothermal conditions were characterized by XRD, IR and Raman spectra.

Key words: INFRARED SPECTROPHOTOMETRY, X-RAY DIFFRACTION ANALYSIS, RAMAN SPECTROMETRY, HYDROTHERMAL METHOD

CLC Number:

O612

Cite this article

WANG HAIZENG;TU KUNGANG;PANG WENQIN. Studies on the hydrothermal synthesis of NaZr~2(AsO~4)~3[J]. Acta Chimica Sinica, 1994, 52(9): 883-887.

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NaZr~2(AsO~4)~3的水热合成研究