Preparation and Characterization of MnOOH Nanorods in Reverse Micelles

Acta Chimica Sinica ›› 2004, Vol. 62 ›› Issue (24): 2441-2443. Previous Articles Next Articles

MnOOH纳米棒的反胶束法制备及表征

董喜燕, 张兴堂, 程纲, 李蕴才, 杜祖亮

河南大学特种功能材料重点实验室, 开封, 475001

投稿日期:2004-04-12 修回日期:2004-05-25 发布日期:2014-02-17
通讯作者: 杜祖亮,E-mail:zld@henu.edu.cn E-mail:zld@henu.edu.cn
基金资助:
国家自然科学基金(Nos.20371015,90306010)和"973"前期专项(No.2002CCC02700)资助项目.

Preparation and Characterization of MnOOH Nanorods in Reverse Micelles

DONG Xi-Yan, ZHANG Xing-Tang, CHENG Gang, LI Yun-Cai, DU Zu-Liang

Key Laboratory for Special Functional Materials, Henan University, Kaifeng 475001

Received:2004-04-12 Revised:2004-05-25 Published:2014-02-17

Abstract

MnOOH nanorods were synthesized in quaternary water/oil (W/O) microemulsion solution containing CTAB, n-butanol, heptane and water. Transmission electron microscopy (TEM) and high resolution transmission electron microscopy (HRTEM), electron diffraction analysis (ED) and X-ray diffraction (XRD) were utilized to characterize the shape, size and structure of the obtained products. The results show that the nanorods were monoclinic manganese oxyhydroxide, which were about 10 nm in diameter and more than 200 nm in length. Moreover, the length of nanorods increased with the increase of reacting time, while the diameter had no change.

Key words: MnOOH nanorod, CTAB, reverse micelle

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DONG Xi-Yan, ZHANG Xing-Tang, CHENG Gang, LI Yun-Cai, DU Zu-Liang. Preparation and Characterization of MnOOH Nanorods in Reverse Micelles[J]. Acta Chimica Sinica, 2004, 62(24): 2441-2443.

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[1] Bach, S.; Henry, M.; Baffier, N.; Livage, J. J. Solid State Chem. 1900, 88, 325.
[2] Bach, S.; Pereira-Ramos, J. P.; Baffier, N.; Messina, R. Electrochim. Acta 1991, 36, 1595.
[3] Hunter, J. J. Solid State Chem. 1981, 39, 142.
[4] Bach, S.; Ramos, P.; Baer, N. J. Solid State Chem. 1995, 120, 70.
[5] Al-Sagheer, F. A.; Zaki, M. I. Colloid Surface A 2000, 173, 193.
[6] Kanasaku, K.; Amezawa, N. Solid State Ionics 2000, 133, 51.
[7]
[8]
[9] Wang, X.; Li, Y.-D. Chem. Commun. 2002, 764.
[10] Wang, X.; Li, Y.-D. J. Am. Chem. Soc. 2002, 124, 2881.
[11] Xiong, Y.-J.; Xie, Y. Chem. Eur. J. 2003, 9, 1645.
[12] Yi, T.; Gao, S.; Qi, X.; Zhu, Y.-F.; Huang, Y.-H.; Cheng, F.-X.; Liao, C.-S.; Yan, C.-H. Acta Chim. Sinica 2000, 58, 162 (in Chinese).(易涛, 高松, 戚星, 朱永法, 黄云辉, 程福祥, 廖春生, 严纯华, 化学学报, 2000, 58, 162.)
[13] Wang, W.-Z.; Xu, C.-K.; Wang, G.-H.; Liu, Y.-K.; Zheng, C.-L. Adv. Mater. 2002, 14, 837.
[14] Sharma, P. K.; Whittingham, M. S. Mater. Lett. 2001, 48, 319.
[15] Ocana, M. Colloid Polym. Sci. 2000, 278, 443.
[16] Sharma, P. K.; Whittingham, M. S. Mater. Lett. 2001, 48, 319.
[17] Zhou, W.-L.; Kumbhar, A.; Wiemann, J.; Fang, J.-Y.; Carpenter, E. E.; O'Connor, C. J. J. Solid State Chem. 2001, 159, 26.
[18] Zhou, H.-C.; Zhuang, J.; Wang, X.; Xu, J.; Li, Y.-D. Acta Chim. Sinica 2003, 61, 372 (in Chinese).(周海成, 庄京, 王训, 徐建, 李亚栋, 化学学报, 2003, 61, 372.)
[19] Maillard, M.; Otte, L.; Ngo, A. T.; Pileni, M. P. J. Phys. Chem. B 2000, 104, 871.
[20] Palazzo, G.; Lopez, F.; Giustini, M.; Colafemmina, G.; Ceglie, A. J. Phys. Chem. B 2003, 107, 1924.
[21] Plazzo, G.; Carbone, L.; Colafemmina, G.; Angelico, R.; Ceglie, A.; Giustini, M. Phys. Chem. Chem. Phys. 2004, 6(7), 1423.
[22] Giovanoli, R.; Leuenberger, V. Chim. Acta 1969, 52, 2333.

MnOOH纳米棒的反胶束法制备及表征

Preparation and Characterization of MnOOH Nanorods in Reverse Micelles

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