Acta Chimica Sinica ›› 2003, Vol. 61 ›› Issue (3): 372-375. Previous Articles     Next Articles

Original Articles

反相胶束法控制合成不同形貌半导体Ag_2S纳米晶

周海成;庄京;王训;徐建;李亚栋   

  1. 清华大学化学系
  • 发布日期:2003-03-15

Synthesis and Characterization of Ag2S Nanocrystals with Different Morphologies in Micromicelles

Zhou Haicheng;Zhuang Jing;Wang Xun;Xu Jian;Li Yadong   

  1. Department of Chemistry,Tsinghua University
  • Published:2003-03-15

Semiconductor Ag_2S nanocrytsals with different morphologies were synthesized in quaternary W/0 microemulsion solution containing Triton X-100, cyclohexane and n-pentanol. And particularly, the synthesis of AgjS nanorods with lengths up to 2.0-3.5 /uun and aspect ratio of 20 - 70 has been reported for the first time. The reaction conditions were optimized through investigations on the influences of W_0 , the concentration of the reactant, and the aging time on the morphology and the sizes of the products. Transmission electron microscopy (TEM) was utilized to characterize the shape and size of the obtained products.

Key words: Ag_2S, NANOPHASE MATERIALS, MICELLE, CYCLOHEXANE, PENTANOL, STRUCTURE CHARACTERISTICS

CLC Number: