The study of tetraaza [14] annulene nickel (Ⅱ) compounds 3: Preparation, characterization and electrochemical behaviors of substituted tetraaza [14] annulene nickel (Ⅱ) and the corresponding tricarbonyl chromium heteropolynuclear complexes

Acta Chimica Sinica ›› 1997, Vol. 55 ›› Issue (2): 160-166. Previous Articles Next Articles

Original Articles

四氮[14]轮烯合镍(Ⅱ)配合物的研究 3: 取代四氮[14]轮烯合镍(Ⅱ)及其π配位三羰基合铬多核配合物的合成、表征及电化学性质

章文伟;孟庆金;许尔杰;游效曾

南京大学配位化学研究所

发布日期:1997-02-15

The study of tetraaza [14] annulene nickel (Ⅱ) compounds 3: Preparation, characterization and electrochemical behaviors of substituted tetraaza [14] annulene nickel (Ⅱ) and the corresponding tricarbonyl chromium heteropolynuclear complexes

ZHANG WENWEI;MENG QINGJIN;XU ERJIE;YOU XIAOZENG

Published:1997-02-15

Abstract

Four new heteropoly nuclear complexes have been synthesized by the reaction of hexacarbonyl chromium with the tetraaza [14] annulene nickel (Ⅱ) macrocycles, which have very special structure. All of them have been characterized via EA, IR, UV, ^1H NMR, ^1^3C NMR, MS. The electrochemical behaviors of these compounds have also been studied by clclic voltammetry.

Key words: ULTRAVIOLET SPECTROPHOTOMETRY, INFRARED SPECTROPHOTOMETRY, MOLECULAR STRUCTURE, PROTON MAGNETIC RESONANCE SPECTROMETRY, CARBONYL COMPOUNDS, CHROMIUM COMPOUNDS, NICKEL COMPLEX, ANNULENE

CLC Number:

O611.662

Cite this article

ZHANG WENWEI;MENG QINGJIN;XU ERJIE;YOU XIAOZENG. The study of tetraaza [14] annulene nickel (Ⅱ) compounds 3: Preparation, characterization and electrochemical behaviors of substituted tetraaza [14] annulene nickel (Ⅱ) and the corresponding tricarbonyl chromium heteropolynuclear complexes[J]. Acta Chimica Sinica, 1997, 55(2): 160-166.

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四氮[14]轮烯合镍(Ⅱ)配合物的研究 3: 取代四氮[14]轮烯合镍(Ⅱ)及其π配位三羰基合铬多核配合物的合成、表征及电化学性质

The study of tetraaza [14] annulene nickel (Ⅱ) compounds 3: Preparation, characterization and electrochemical behaviors of substituted tetraaza [14] annulene nickel (Ⅱ) and the corresponding tricarbonyl chromium heteropolynuclear complexes

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