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Acta Chimica Sinica ›› 1964, Vol. 30 ›› Issue (2): 233-236. Previous Articles Next Articles
吴钧和, 董庭威, 章道道, 王新民, 孙熊鸣
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OU KIUN-HOUO, TONG TING-WEI, CHANG TAO-TAO, WANG SIN-MIN, SUN YUNG-MIN
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Fifteen N-substituted compounds of O,O-dimethyl S-(carbamoylmethyl) phosphorodithioate were prepared by two methods A and B.Method A was based on the reaction of O,O-dimethyl phosphorodithioate and N-substituted α-choroacetylamide in the presence of sodium carbonate in acetone as solvent.In method B the reaction of the sodium salt of the O,O-dimethyl phosphorodithioate and N-substituted α-chloroacetylamide was carried out.The structural formulas,melting points,elementary analyses and the solvents for recrystallization of these compounds were listed in the Table (in Chinese text).
OU KIUN-HOUO, TONG TING-WEI, CHANG TAO-TAO, WANG SIN-MIN, SUN YUNG-MIN. SYNTHESIS OF SOME N-SUBSTITUTED O, O-DIMETHYL S-(CARBAMOYL-METHYL) PHOSPHORODITHIOATES[J]. Acta Chimica Sinica, 1964, 30(2): 233-236.
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