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Acta Chimica Sinica ›› 1956, Vol. 22 ›› Issue (6): 507-512. Previous Articles     Next Articles

氮大圜化合物的合成——Ⅰ.2-异丙基-5-甲基氮七圜的衍生物

陆启荣1,2, F. F. Blicke1,2   

  1. 1. 广州中山大学化学系;
    2. 密歇根大学药学系
  • 投稿日期:1956-08-06 发布日期:2013-06-03

SYNTHESIS OF LARGE-MEMBERED NITROGENOUS RING COMPOUNDS—Ⅰ.DERIVATIVES OF 2-ISOPROPYL-5-METHYLHEXAMETHYLENIMINE

LU CHI-JUNG1,2, F. F. BLTCKE1,2   

  1. 1. Department of Chemistry, Sun Yat-Sen University;
    2. College of Pharmacy, University of Michigan
  • Received:1956-08-06 Published:2013-06-03

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2-Isopropyl-5-methyl-7-ketohexamethylenimine was prepared by a process starting with menthol, very similar to that described by Wallach in 1893. By the use of lithium aluminum hydride, the laUam was reduced to 2-isopropyl-5-methyl-hexamethylenimine.