In-situ Etching Strategy for Manipulation of Hierarchical Zeolite and Its Application★
Received date: 2023-04-28
Online published: 2023-07-07
Supported by
National Natural Science Foundation of China(21972006); Shenzhen Science and Technology Program(JCYJ20200109140421071); Shenzhen Science and Technology Program(JSGG20211029095546003)
Zeolite molecular sieve is by far the most widely used porous material with the greatest contribution to society. Hierarchical zeolites, which possess dual advantages of large diffusion coefficient and high activity, are increasingly important as catalysts and adsorbents in many chemical processes. A class of organic mesoporogens named organic mesopore generating agents (OMeGAs), such as amino acids, phenols, and azoles were found to produce intracrystalline mesopores by one pot method, wherein the nucleophilic etching effect of the in-situ generated anions, including oxyanions, nitranions, or carbanions, plays the key role. By adding mild OMeGAs in-situ into the reaction solution of zeolite synthesis, the nucleophilic etching assisted growth could overcome the energy-intensive mesoscale template calcination associated with the “bottom-up” strategy and the zeolite structure destruction of the “top-down” post-synthetic strategy. The interplay between in-situ etching and growth on the early precursor or nuclei has enabled effective control over crystallinity, size, morphology, mesopores, and performance of zeolites. In this account, the existing preparation strategies of hierarchical zeolite are first briefly introduced. Then, the in-situ etching-assisted growth strategies are discussed in detail, including the selection of mild etchant OMeGAs, mechanism and advantages of the etching-assisted zeolite crystallization process. Finally, the application of in-situ etching-manipulated hierarchical zeolite is summarized.
Mei Hong , Jinqiang Gao , Tong Li , Shihe Yang . In-situ Etching Strategy for Manipulation of Hierarchical Zeolite and Its Application★[J]. Acta Chimica Sinica, 2023 , 81(8) : 937 -948 . DOI: 10.6023/A23040177
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