Studies on derivatives of the thiophosphoryl ureas VI: N-(O-alkyl-O-arylthiophosphoryl)-N'-aroylurea

Chin. J. Org. Chem. ›› 1989, Vol. 9 ›› Issue (2): 176-180. Previous Articles

硫代磷酰脲衍生物的研究 VI: N-(O-烷基-O-芳基硫代磷酰基)-N'-芳酰基脲

刘钊杰;胡汉斌;张景龄

华中师范大学有机合成研究所

发布日期:1989-04-25

Studies on derivatives of the thiophosphoryl ureas VI: N-(O-alkyl-O-arylthiophosphoryl)-N'-aroylurea

LIU ZHAOJIE;HU HANBIN;ZHANG JINGLING

Published:1989-04-25

Abstract

Refluxing RC6H4CONH2 (R = H, 4-Cl, 2-NO2) with oxalyl chloride followed by treatment of RC6H4CONCO with R1C6H4OP(S)(OR2)NH2 (R1 = H, 2-, 3-, 4-Me, 4-Cl, 3-, 5-NO2, 2-CO2CHMe2; R2 = Me, Et, Pr, Me2CH, Bu, Me2CHCH2, amyl, isoamyl) gave 58.5-96.8% the title compounds I.

Key words: INFRARED SPECTROPHOTOMETRY, ELEMENTAL ANALYSIS, ORGANO PHOSPHORUS COMPOUNDS, PHOSPHORYL COMPOUNDS, PROTON MAGNETIC RESONANCE SPECTROMETRY, PHOSPHORAMIDOTHIOIC ACID P, UREAS, ISOCYANATE

CLC Number:

O621

Cite this article

LIU ZHAOJIE;HU HANBIN;ZHANG JINGLING. Studies on derivatives of the thiophosphoryl ureas VI: N-(O-alkyl-O-arylthiophosphoryl)-N'-aroylurea[J]. Chin. J. Org. Chem., 1989, 9(2): 176-180.

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硫代磷酰脲衍生物的研究 VI: N-(O-烷基-O-芳基硫代磷酰基)-N'-芳酰基脲

Studies on derivatives of the thiophosphoryl ureas VI: N-(O-alkyl-O-arylthiophosphoryl)-N'-aroylurea

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