Chin. J. Org. Chem. ›› 1993, Vol. 13 ›› Issue (1): 61-63. Previous Articles     Next Articles

Original Articles

2-羟基-5-甲基-5-(4-甲基戊烯-3-)基四氢呋喃的合成

徐宝财;柯友之;徐锡瑛   

  1. 北京轻工业学院化学工程系
  • 发布日期:1993-02-25

Synthesis of 2-hydroxy-5-methyl-5-(4-methylpenten-3-)tetrahydrofuran

XU BAOCAI;KE YOUZHI;XU XIYING   

  • Published:1993-02-25

A grignard reaction of a bromodioxolane (1) with 6-methylhepten-5-one-2 was followed by hydrolysis with aqueous NH4CL to give a hydroxydioxolane (3).hydrolysis of 3 with TSOH yield a hydroxytetrahydrofuran(4), 3 and 4 have not been reported in the literature and were characterized by elemental analysis.IR HNMR , MS and GC-MS.3 and 4 are found to be potential perfume compounds.

Key words: PENTENE P, PERFUMES, TETRAHYDROFURAN P

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