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Chin. J. Org. Chem. ›› 1993, Vol. 13 ›› Issue (1): 61-63. Previous Articles Next Articles
Original Articles
徐宝财;柯友之;徐锡瑛
发布日期:
XU BAOCAI;KE YOUZHI;XU XIYING
Published:
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A grignard reaction of a bromodioxolane (1) with 6-methylhepten-5-one-2 was followed by hydrolysis with aqueous NH4CL to give a hydroxydioxolane (3).hydrolysis of 3 with TSOH yield a hydroxytetrahydrofuran(4), 3 and 4 have not been reported in the literature and were characterized by elemental analysis.IR HNMR , MS and GC-MS.3 and 4 are found to be potential perfume compounds.
Key words: PENTENE P, PERFUMES, TETRAHYDROFURAN P
CLC Number:
O651
XU BAOCAI;KE YOUZHI;XU XIYING. Synthesis of 2-hydroxy-5-methyl-5-(4-methylpenten-3-)tetrahydrofuran[J]. Chin. J. Org. Chem., 1993, 13(1): 61-63.
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