Synthesis and characterization of Fe(η^5-C5H4S)2M(η^5-C5H5)Cl

Chin. J. Org. Chem. ›› 1996, Vol. 16 ›› Issue (3): 270-273. Previous Articles Next Articles

Original Articles

铁双(双戊二烯巯基)环戊二烯基钛(Ⅳ), 锆(Ⅳ)的合成和结构表征

刘楚圣;周耀坤

抚顺石油化工研究院;兰州大学化学系

发布日期:1996-06-25

Synthesis and characterization of Fe(η^5-C5H4S)2M(η^5-C5H5)Cl

LIU CHUSHENG;ZHOU YAOKUN

Published:1996-06-25

Abstract

Two new metallsdithiaferrocencophanes of type Fe(η^5-C5H4S)2MCl(η^5-C5H5)(M=Tim Zr) have been prepared by the reaction of ferrocene -1, 1'-dithiol with bis ((5-Cyclopentadienyl) Titanium (Ⅳ) dichloride, bis(η^5-Cyclopentadienyl) Zirconium (Ⅳ) dichloride respectively in anhydrous benzene under the present of sodium amide. The composition and structure of compounds 5 and 6 have been characterized by elemental analysis, IR and ^1H NMR.

Key words: PROTON MAGNETIC RESONANCE SPECTROMETRY, STRUCTURE CHARACTERISTICS, INFRARED SPECTROPHOTOMETRY

CLC Number:

O627

Cite this article

LIU CHUSHENG;ZHOU YAOKUN. Synthesis and characterization of Fe(η^5-C5H4S)2M(η^5-C5H5)Cl[J]. Chin. J. Org. Chem., 1996, 16(3): 270-273.

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铁双(双戊二烯巯基)环戊二烯基钛(Ⅳ), 锆(Ⅳ)的合成和结构表征

Synthesis and characterization of Fe(η^5-C5H4S)2M(η^5-C5H5)Cl

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