Chin. J. Org. Chem. ›› 2002, Vol. 22 ›› Issue (2): 135-137. Previous Articles     Next Articles

4-甲氧基-2,3,5-三甲基吡啶的合成新方法

刘田春;吕秀阳;吴平东   

  1. 浙江大学材料与化工学院,杭州(310027)
  • 发布日期:2002-02-25

A new method for the synthesis of 4-methoxyl-2,3,5- trimethylpyridine

Liu Tianchun;Lu Xiuyang;Wu Pingdong   

  1. College of Material Science and Chemical Engineering, Zhejiang University,Hangzhou(310027)
  • Published:2002-02-25

A new and efficient method for the synthesis of 4-methoxyl-2,3,5- trimethylpyridine with an overall yield of 76% from cheap and easily available 2, 3, 5-trimethylpyridine was developed. The structure of related compounds was identified by IR, ~1H NMR and ~(13)C NMR. The method could be carried out economically on a large scale.

Key words: TRIMETHYL GROUP;PYRIDINE P;DEOXIDIZATION;SYNTHESIS, INFRARED SPECTROSCOPY;NUCLEAR MAGNETIC RESONANCE

CLC Number: