Clean Synthesis of 2-Amino-3-cyano-4-aryl-7,7-dimethyl-5-oxo-4H-5,6, 7,8-tetrahydrobenzo[b] pyran in Water

Chin. J. Org. Chem. ›› 2003, Vol. 23 ›› Issue (8): 877-879. Previous Articles Next Articles

水中2-氨基-3-氰基-4-芳基-7，7-二甲基-5-氧代4H-5，6，7，8-四氢苯并[b]吡喃的洁净合成

史达清;张姝;庄启亚;屠树江;胡宏纹

徐州师范大学化学系;南京大学化学系

发布日期:2003-08-25

Clean Synthesis of 2-Amino-3-cyano-4-aryl-7,7-dimethyl-5-oxo-4H-5,6, 7,8-tetrahydrobenzo[b] pyran in Water

Shi Daqing;Zhang Shu;Zhuang Qiya;Tu Shujiang;Hu Hongwen

Department of Chemistry, Xuzhou Normal University;Department of Chemistry, Nanjing University

Published:2003-08-25

Abstract

CLC Number:

O621

Cite this article

Shi Daqing;Zhang Shu;Zhuang Qiya;Tu Shujiang;Hu Hongwen. Clean Synthesis of 2-Amino-3-cyano-4-aryl-7,7-dimethyl-5-oxo-4H-5,6, 7,8-tetrahydrobenzo[b] pyran in Water[J]. Chin. J. Org. Chem., 2003, 23(8): 877-879.

[1]	ZHANG Mei-Mei, LI Qiang, TUN Jian-Rong, WANG Xiang-Shan. A Clean Synthesis of 1,4-Diarylquinoline-2,5-dione Derivatives in Aqueous Media [J]. Chin. J. Org. Chem., 2009, 29(11): 1811-1815.
[2]	ZHUANG Qi-Ya,b,WU Nan^a,SHI Da-Qing*^,a,b TU Shu-Jiang,b,WANG Xiang-Shan,b. Synthesis of 2-Amino-3-cyano-4-aryl-7,7-dimethyl-5-oxo-4H-5,6,7,8- tet-rahydrobenzo[b]pyran Catalyzed by KF-Montmorillonite [J]. Chin. J. Org. Chem., 2006, 26(9): 1217-1220.
[3]	LIU Gang^1,2,ZHANG Rong-Li,CAI Ming-Zhong*^,1. Synthesis and Catalytic Characteristics of a Silica-Supported Poly-ω-(methylseleno)undecylsiloxane Palladium(0) Complex [J]. Chin. J. Org. Chem., 2006, 26(02): 215-218.
[4]	WANG Xiang-Shan*^,1,2,3,ZENG Zhao-Sen^1,3,LI Yu-Ling^1,3,SHI Da-Qing^1,3 TU Shu-Jiang^1,3,WEI Xian-Yong²,ZONG Zhi-Min². Synthesis of 2-Amino-4-aryl-5,6-dihydro-4H-pyrano[3,2-c]quinolin-5-one Derivatives in Water [J]. Chin. J. Org. Chem., 2006, 26(02): 228-232.
[5]	WANG, Xiang-Shan, SHI, Da-Qing, ZHANG, Yan-Fei, WANG, Su-Hui, TU, Shu-Jiang. Synthesis of 9-Arylpolyhydroacridine in Water Catalyzed by Triethylbenzylammonium Chloride (TEBA) [J]. Chinese Journal of Organic Chemistry, 2004, 24(4): 430-432.
[6]	Shi Daqing;Zhang Shu;Zhuang Qiya;Tu Shujiang;Hu Hongwen. Michael Addition of 3-Methyl-1-phenyl-2-pyrazolin-5-one to α,β- Unsaturated Ketones in Water [J]. Chin. J. Org. Chem., 2003, 23(9): 1036-1038.
[7]	Shi Daqing;Zhang Shu;Zhuang Qiya;Tu Shujiang;Hu Hongwu. Reaction of Substituted Cinnamonitriles with β-Naphthol in Water [J]. Chin. J. Org. Chem., 2003, 23(8): 809-812.
[8]	Shi Daqing;Zhuang Qiya;Chen Jing;Wang Xiangshan;Tu Shujiang;Hu Hongwen. Reaction of Aromation Aldehydes with 5,5-Diemthyl-1,3- cyclohexandione in Water [J]. Chin. J. Org. Chem., 2003, 23(7): 694-696.
[9]	Tu Shujiang;Jiang Hong;Zhuang Qiya;Miao Chunbao;Shi Daqing;Wang Xiangshan;Gao Yuan. One-Pot Synthesis of 2-Amimo-3-cyano-4-aryl-7,7-dimethyl-5-oxo-5,6, 7,8-tetrahydro-4H-benzo[b]pyran under Ultrasonic Irradiation without Catalyst [J]. Chin. J. Org. Chem., 2003, 23(5): 488-490.
[10]	Shi Daqing;Zhang Shu;Zhuang Qiya;Wang Xiangshan;Tu Shujiang;Hu Hongwen. Clean Synthesis of Benzo[ h ]chromene Derivatives in Water [J]. Chin. J. Org. Chem., 2003, 23(12): 1419-1421.
[11]	Shi Daqing;Zhang Shu;Zhang Qiya;Tu Shujiang;Hu Hongwen. Clean Synthesis of 3-Methyl-6-amino-5-cyano-4-aryl-1-phenyl-1,4- dihydropyrano[2,3-c]pyrazole in Water [J]. Chin. J. Org. Chem., 2003, 23(11): 1314-1316.
[12]	Gao Yuan;Tu Shujiang;Zhou Jianfeng;Shi Daqing. A convenient synthesis of 2-amino-5,6,7,8-tetrahydro-5-oxo-4-aryl- 7, 7-dimethyl-4H-benzo-[b]-pyran-3-ethylcarboxylates without catalyst [J]. Chin. J. Org. Chem., 2001, 21(7): 535-537.
[13]	Wu Chengtai;He Yongbing;Fu Enqin. Studies on azacrown ether compounds and macrocyclic polyamines [J]. Chin. J. Org. Chem., 2001, 21(11): 914-922.
[14]	Zhou Jianfeng;Tu Shujiang;Gao Yuan;Ji Ming. One pot synthesis of pyrans and pyrano[2, 3-c] pyrazole derivatives under microwave irradiation [J]. Chin. J. Org. Chem., 2001, 21(10): 742-745.
[15]	SUN HONGBIN;HUA WEIYI;CHEN LING;PENG SIXUN. Synthesis of 7,8-dihydro-6,6-dimethyl-7,8-epoxy-6H-pyrano[2,3-f] benzo-2,1,3-oxadiazole [J]. Chin. J. Org. Chem., 1997, 17(6): 547-550.

水中2-氨基-3-氰基-4-芳基-7，7-二甲基-5-氧代4H-5，6，7，8-四氢苯并[b]吡喃的洁净合成

Clean Synthesis of 2-Amino-3-cyano-4-aryl-7,7-dimethyl-5-oxo-4H-5,6, 7,8-tetrahydrobenzo[b] pyran in Water

PDF

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments