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Chin. J. Org. Chem. ›› 2005, Vol. 25 ›› Issue (11): 1469-1472. Previous Articles Next Articles
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赵莹*,谭晓燕,杨志,李姣娟
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ZHAO Ying*,TAN Xiao-Yan,YANG Zhi,LI Jiao-Juan
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In this paper, methyl-N,N-bis(2-cyanoethyl)aniline was synthesized by the reaction of o-methylaniline, m-methylaniline or p-methylaniline with acrylonitrile in the present of AlCl3 or AlCl3-ZnCl2. The experimental results proved that AlCl3 was an excellent catalyst, and AlCl3-ZnCl2 was better than AlCl3 in catalyzing this reaction, and the yields of m- and p-products were 92%~94%.
Key words: methyl-N,N-bis(2-cyanoethyl)aniline, ZnCl2, AlCl3
ZHAO Ying*,TAN Xiao-Yan,YANG Zhi,LI Jiao-Juan. Synthesis of Methyl-N,N-bis(2-cyanoethyl)aniline Catalyzed by AlCl3[J]. Chin. J. Org. Chem., 2005, 25(11): 1469-1472.
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