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Chin. J. Org. Chem. ›› 2005, Vol. 25 ›› Issue (12): 1580-1582. Previous Articles     Next Articles

Reports

E-3-二茂铁基-2-丙烯醛的简便合成方法

连小春，杜计燕，温孟赢，孙真荣，汤杰*   

  1. (1华东师范大学化学系 上海 200062)
    (2华东师范大学光谱学与波谱学教育部重点实验室 上海 200062)
  • 收稿日期:2005-01-20 修回日期:2005-06-02 发布日期:2005-11-30
  • 通讯作者: 汤杰

Practical Preparation of E-3-Ferrocenyl-2-propenal Using Diethyl 2-(Cyclohexylamino)vinylphosphonate

LIAN Xiao-Chun, DU Ji-Yan, WEN Meng-Ying, SUN Zhen-Rong, TANG Jie*   

  1. (1 Department of Chemistry, East China Normal University, Shanghai 200062)
    (2 Key Laboratory of Optical and Magnetic Resonance Spectroscopy, Ministry of Education,
    East China Normal University, Shanghai 200062)
  • Received:2005-01-20 Revised:2005-06-02 Published:2005-11-30
  • Contact: TANG Jie

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A practical procedure for preparation of E-3-ferrocenyl-2-propenal was developed from ferrocene carboxaldehyde and Nagata’s reagent to provide the target product in high yield under mild conditions.

Key words: E-3-ferrocenyl-2-propenal, ferrocene carboxaldehyde, Wittig-Horner reaction, Nagata’s reagent