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Chin. J. Org. Chem. ›› 2003, Vol. 23 ›› Issue (3): 265-269. Previous Articles     Next Articles

三种尾式卟啉的合成及结构表征

李早英;王凯;赵一玫;李洪阳   

  1. 武汉大学化学与分子科学学院;红桃K集团股份有限公司研究院
  • 发布日期:2003-03-25

Synthesis and Structural Characterization of Three Tailed Porphyrins

Li Zaoying;Wang,Kai;Zhao YiMei;Li Hongyang   

  1. College of Chemistry and Molecular Sciences,Wuhan University;Institute of RHK(Group)Co.,Ltd.,
  • Published:2003-03-25

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The reaction of 5-(4-hydroxyphenyl)-10,15,20-tris(4-methoxyphenyl) porphyrin (1) with acetylsalicyloyl chloride gave compound 3. Treatment of 5-(4-bromobutyloxyphenyl)-10, 15, 20-tris(4-methoxyphenyl)porphyrin (2) with phenylpiperazine and l-(4-methoxyphenyl)piperazine produced compounds 4 and 5, respectively. The structures of new compounds were confirmed by absorption spectroscopy, H NMR, MS and elemental analysis.

Key words: ASPIRIN;PIPERAZINE P;PORPHYRIN;STRUCTURE CHARACTERISTICS, 1HNMR;MS;ELEMENTAL ANALYSIS

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