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Chin. J. Org. Chem. ›› 2003, Vol. 23 ›› Issue (8): 846-849. Previous Articles Next Articles
李人宇;卑凤利;马卫兴;杨绪杰;许兴友;陆路德;汪信
发布日期:
Li Renyu;Bei Fengli;Ma Weixing;Yang Xujie;Xu Xingyou;Lu Lude;Wang Xin
Published:
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N-Salicylidene-4-aminoantipyrine was synthesized by the solid phase reaction of 4-aminoantipyrine with salicylaldehyde at room temperature without solvent. The reaction was completed in 15 min in 95% yield. The product was characterized by elemental analysis, IR, *H NMR, X-ray powder diffraction and X-ray single crystal diffraction.
Key words: ANTIPYRINU;SCHIFF BASE;ELEMENTAL ANALYSIS;IR;1HNMR;XRD, STRUCTURE CHARACTERISTICS
CLC Number:
O621
Li Renyu;Bei Fengli;Ma Weixing;Yang Xujie;Xu Xingyou;Lu Lude;Wang Xin. One Step Sysnthesis of N-Salicylidene-4-aminoantipyrine by Solid Phase Reaction at Room Temperature[J]. Chin. J. Org. Chem., 2003, 23(8): 846-849.
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