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Chin. J. Org. Chem. ›› 2009, Vol. 29 ›› Issue (08): 1264-1266. Previous Articles Next Articles
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郭 建; 庄 顺; 陈松华; 张士博; 袁耀锋*
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Guo, Jian ; Zhuang, Shun; Chen, Songhua; Zhang, Shibo; Yuan, Yaofeng*
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Ferrocenecarboxaldehyde is an important intermediate in organic synthetic chemistry. The application of 1’-substituted ferrocenecarboxaldehyde is limited because of the difficulty of synthesis. Due to many reactive sites, 1’-iodoferrocenecarboxaldehyde was widely used in the design and synthesis of functional molecules. The traditional synthetic methods not only require four steps, but also need to use expensive metal-organic reagents. 1’-Iodoferrocenecarboxaldehyde has been prepared from ferrocene through an improved three-step procedure, which features ready availability of the starting materials and simple opera-tion.
Key words: Vilsmeier formylation, l’-iodoferrocenecarbaldehyde, ferrocene derivative
Guo, Jian ; Zhuang, Shun; Chen, Songhua; Zhang, Shibo; Yuan, Yaofeng* . A New Route for the Synthesis of l’-Iodoferrocenecarboxaldehyde[J]. Chin. J. Org. Chem., 2009, 29(08): 1264-1266.
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