The synthesis of 5-butyl-9-phenyl-4, 5, 6, 9-tetraydrobenzo[d.e]- oxazolo[5, 4-g]-isoquinoline-4, 6-dinones

Chin. J. Org. Chem. ›› 1995, Vol. 15 ›› Issue (6): 633-637. Previous Articles Next Articles

Original Articles

5-丁基-9-苯基-4, 5, 6, 9-四氢苯并[d, e]恶唑[5, 4-g]-异喹啉-4, 6-二酮的合成

柳波;沈永嘉;倪彩英;董黎芬

华东理工大学精细化工研究所

发布日期:1995-12-25

The synthesis of 5-butyl-9-phenyl-4, 5, 6, 9-tetraydrobenzo[d.e]- oxazolo[5, 4-g]-isoquinoline-4, 6-dinones

LIU BO;SHEN YONGJIA;DONG LIFEN

Published:1995-12-25

Abstract

N-butyl-3-amino-4-hydroxyl-1, 8-naphthalimine was synthesized from 4-bromo-1, 8-naphthalic anhydride via the reaction of imination, nitration, hydrolysis and reduc-tion. The better reaction route was given. It can react with benzoyl chloride in the presence of bor-ic acid and form the title compound. The Mass, ^1H NMR, IR and UV spectra of the compound were given.

Key words: ULTRAVIOLET SPECTROPHOTOMETRY, INFRARED SPECTROPHOTOMETRY, ISOQUINOLINE P, MASS SPECTROGRAPHY, CHROMOPHOR, NMR SPECTROMETRY

CLC Number:

O621

Cite this article

LIU BO;SHEN YONGJIA;DONG LIFEN. The synthesis of 5-butyl-9-phenyl-4, 5, 6, 9-tetraydrobenzo[d.e]- oxazolo[5, 4-g]-isoquinoline-4, 6-dinones[J]. Chin. J. Org. Chem., 1995, 15(6): 633-637.

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5-丁基-9-苯基-4, 5, 6, 9-四氢苯并[d, e]恶唑[5, 4-g]-异喹啉-4, 6-二酮的合成

The synthesis of 5-butyl-9-phenyl-4, 5, 6, 9-tetraydrobenzo[d.e]- oxazolo[5, 4-g]-isoquinoline-4, 6-dinones

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