share
Chin. J. Org. Chem. ›› 2008, Vol. 28 ›› Issue (08): 1428-1432. Previous Articles Next Articles
Original Articles
尹红星a; 张殊佳 a,b ; 郑学仿*,b; 杨兰义a
收稿日期:
修回日期:
发布日期:
通讯作者:
YIN, Hong-Xing a; ZHANG, Shu-Jia a,b; ZHENG, Xue-Fang*,b ; YANG, Lan-Yia
Received:
Revised:
Published:
Contact:
Share
A convenient and efficient procedure is described for the preparation of β-elemene-13-yl alkyl selenides by treatment of selenium with N2H48226;H2O/RX/NaBH4/13-chloro-β-elemene sequentially in one-pot at room temperature. This method has several advantages such as simple operation, short reaction time, mild conditions and high yields. It also provides a convenient and efficient way to the synthesis of unsymmetrical dialkyl selenides. The preliminary bioassay showed that product g exhibited notable antioxidation activity.
Key words: β-elemene, one-pot procedure, antioxidation, unsymmetrical selenide
YIN, Hong-Xing a; ZHANG, Shu-Jia a,b; ZHENG, Xue-Fang*,b ; YANG, Lan-Yia. One-Pot Synthesis of β-Elemene-13-yl Alkyl Selenides[J]. Chin. J. Org. Chem., 2008, 28(08): 1428-1432.
Export EndNote|Reference Manager|ProCite|BibTeX|RefWorks