Chinese Journal of Organic Chemistry ›› 2021, Vol. 41 ›› Issue (6): 2290-2301.DOI: 10.6023/cjoc202102051 Previous Articles Next Articles
Special Issue: 有机光催化虚拟合辑; 热点论文虚拟合集
ARTICLES
刘宇a,b, 陈赞a, 陈镤a, 熊碧权a, 谢军a,*(), 刘岸a,*(
), 梁云b, 唐课文a
收稿日期:
2021-02-27
修回日期:
2021-03-18
发布日期:
2021-03-25
通讯作者:
谢军, 刘岸
基金资助:
Yu Liua,b, Zan Chena, Pu Chena, Biquan Xionga, Jun Xiea(), An Liua(
), Yun Liangb, Kewen Tanga
Received:
2021-02-27
Revised:
2021-03-18
Published:
2021-03-25
Contact:
Jun Xie, An Liu
Supported by:
Share
Yu Liu, Zan Chen, Pu Chen, Biquan Xiong, Jun Xie, An Liu, Yun Liang, Kewen Tang. Visible-Light-Catalyzed Tandem Cyanoalkylsulfonylation/ Cyclization of Alkynes[J]. Chinese Journal of Organic Chemistry, 2021, 41(6): 2290-2301.
Entry | Variation from the standard conditions | Yield/% |
---|---|---|
1 | None | 81 |
2 | 2a-1 instead of 2a | 13 |
3 | 2a-2 instead of 2a | 25 |
4 | 2a-3 instead of 2a | 46 |
5 | 2a-4 instead of 2a | 55 |
6 | 2a-5 instead of 2a | 51 |
7 | 2a-6 instead of 2a | 50 |
8 | DABSO instead of K2S2O5 | 8 |
9 | Thiourea dioxide instead of K2S2O5 | 67 |
10c | Na2S2O5 instead of K2S2O5 | 73 |
11c | Without Na2-Eosin Y | 0 |
12 | Ir(ppy)3 instead of Na2-Eosin Y | 59 |
13 | Ru(bpy)3Cl2 instead of Na2-Eosin Y | 34 |
14 | Eosin Y instead of Na2-Eosin Y | 64 |
15 | Without additional light | 0 |
16 | Na2-Eosin Y (5 mol%) | 81 |
17 | Toluene instead of CH3CN | 40 |
18 | THF instead of CH3CN | 38 |
19c | DMF instead of CH3CN | 27 |
20c | Dioxane instead of CH3CN | 44 |
21 | DMSO instead of CH3CN | 32 |
22 | 3 W blue LED light | 61 |
23 | 12 W blue LED light | 54 |
24 | 36 W compact fluorescent light | 45 |
25 | At 100 ℃ | 70 |
26 | At 60 ℃ | 42 |
27 | For 32 h | 80 |
28d | None | 52 |
Entry | Variation from the standard conditions | Yield/% |
---|---|---|
1 | None | 81 |
2 | 2a-1 instead of 2a | 13 |
3 | 2a-2 instead of 2a | 25 |
4 | 2a-3 instead of 2a | 46 |
5 | 2a-4 instead of 2a | 55 |
6 | 2a-5 instead of 2a | 51 |
7 | 2a-6 instead of 2a | 50 |
8 | DABSO instead of K2S2O5 | 8 |
9 | Thiourea dioxide instead of K2S2O5 | 67 |
10c | Na2S2O5 instead of K2S2O5 | 73 |
11c | Without Na2-Eosin Y | 0 |
12 | Ir(ppy)3 instead of Na2-Eosin Y | 59 |
13 | Ru(bpy)3Cl2 instead of Na2-Eosin Y | 34 |
14 | Eosin Y instead of Na2-Eosin Y | 64 |
15 | Without additional light | 0 |
16 | Na2-Eosin Y (5 mol%) | 81 |
17 | Toluene instead of CH3CN | 40 |
18 | THF instead of CH3CN | 38 |
19c | DMF instead of CH3CN | 27 |
20c | Dioxane instead of CH3CN | 44 |
21 | DMSO instead of CH3CN | 32 |
22 | 3 W blue LED light | 61 |
23 | 12 W blue LED light | 54 |
24 | 36 W compact fluorescent light | 45 |
25 | At 100 ℃ | 70 |
26 | At 60 ℃ | 42 |
27 | For 32 h | 80 |
28d | None | 52 |
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