Chinese Journal of Organic Chemistry >
A Red Bayberry Shape Monodisperse Microsphere Support Pd Nanoparticles for Suzuki-Miyaura Cross-Coupling Reaction at Room Temperature
Received date: 2018-03-17
Revised date: 2018-06-08
Online published: 2018-07-16
Supported by
Project supported by the National Undergraduate Training Program for Innovation and Entrepreneurship (No. 201710638031), the Fundamental Research Funds of China West Normal University (No. 17C038) and the Meritocracy Research Funds of China West Normal University (No. 17Y031).
In this study, a controlled synthesis of hyper-crosslinked monodisperse microsphere with homogeneous mesoporous aperture about 6 nm is presented. After supported with palladium, the catalyst was performed by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and nitrogen adsorption and desorption surface area analyses. The results showed that HCP-(PS-DVB)-Pd(0) possessed high catalytic activity for Suzuki-Miyaura cross-coupling reaction at room temperature, and the catalyst also show excellent reusability. After recycled for 10 times, the yield can maintain above 95% and the surface areas can still reach 480.5 m2·g-1. These results suggest that the HCP-(PS-DVB)-Pd(0) catalyst has potential applications in synthetic and industrial chemistry.
Fu Yufang , Zou Zhijuan , Tang Cheng , Song Kunpeng . A Red Bayberry Shape Monodisperse Microsphere Support Pd Nanoparticles for Suzuki-Miyaura Cross-Coupling Reaction at Room Temperature[J]. Chinese Journal of Organic Chemistry, 2018 , 38(11) : 3106 -3111 . DOI: 10.6023/cjoc201803027
[1] Molander, G. A.; Biolatto, B. J. Org. Chem. 2003, 68, 4302.
[2] Zhou, Z.; Zhang, Y.; Xia, W.; Chen, H.; Liang, H.; He, X.; Yu, S.; Cao, R.; Qiu, L. Asian J. Org. Chem. 2016, 5, 1260.
[3] Rathi, A. K.; Gawande, M. B.; Pechousek, J.; Tucek, J.; Aparicio, C.; Petr, M.; Tomanec, O.; Krikavova, R.; Travnicek, Z.; Varma, R. S.; Zboril, R. Green Chem. 2016, 18, 2363.
[4] Fihri, A.; Bouhrara, M.; Nekoueishahraki, B.; Basset, J.-M.; Polshettiwar, V. Chem. Soc. Rev. 2011, 40, 5181.
[5] Martin, R.; Buchwald, S. L. Acc. Chem. Res. 2008, 41, 1461.
[6] Han, F.-S. Chem. Soc. Rev. 2013, 42, 5270.
[7] Amatore, C.; Jutand, A. Acc. Chem. Res. 2000, 33, 314.
[8] Iwai, T.; Tanaka, R.; Harada, T.; Sawamura, M. Chem.-Eur. J. 2014, 20, 1057.
[9] Yamamoto, S. I.; Kinoshita, H.; Hashimoto, H.; Nishina, Y. Nanoscale 2014, 6, 6501.
[10] Boruah, P. R.; Ali, A. A.; Saikia, B.; Sarma, D. Green Chem. 2015, 17, 1442.
[11] Gautam, P.; Dhiman, M.; Polshettiwar, V.; Bhanage, B. M. Green Chem. 2016, 18, 5890.
[12] Song, K.; Liu, P.; Wang, J.; Tan, B.; Li, T. J. Porous Mater. 2016, 23, 725.
[13] Li, B.; Guan, Z.; Wang, W.; Yang, X.; Hu, J.; Tan, B.; Li, T. Adv. Mater. 2012, 24, 3390.
[14] Song, K.; Liu, P.; Wang, J.; Pang, L.; Chen, J.; Hussain, I.; Tan, B.; Li, T. Dalton Trans. 2015, 44, 13906.
[15] Yu, L.; Huang, Y.; Wei, Z.; Ding, Y.; Su, C.; Xu, Q. J. Org. Chem. 2015, 80, 8677.
[16] Liu, Y.; Tang, D.; Cao, K.; Yu, L.; Han, J.; Xu, Q. J. Catal. 2018, 360, 250.
[17] Wang, Q.; Jing, X.; Han, J.; Yu, L.; Xu, Q. Mater. Lett. 2018, 215, 65.
[18] Yu, L.; Han, Z. Mater. Lett. 2016, 184, 312.
[19] Sun, Q.; Dai, Z.; Meng, X.; Xiao, F.-S. Chem. Soc. Rev. 2015, 44, 6018.
[20] Zhou, H.; Wu, C.; Wu, Q.; Guo, B.; Liu, W.; Li, G.; Su, Q.; Mu, Y. Polym. Chem. 2017, 8, 1488.
[21] Wang, C.-A.; Li, Y.-W.; Hou, X.-M.; Han, Y.-F.; Nie, K.; Zhang, J.-P. ChemistrySelect 2016, 1, 1371.
[22] Cheng, T.; Zhijuan, Z.; Yufang, F.; Kunpeng, S. ChemistrySelect 2018, 3, 5987.
[23] Carson, F.; Pascanu, V. A.; Gómez, B.; Zhang , Y.; Platero-Prats, A. E.; Zou, X.; Martín-Matute, B. Chem.-Eur. J. 2015, 21, 10896.
[24] Pascanu, V.; Hansen, P. R.; Bermejo Gómez, A.; Ayats, C.; Platero-Prats, A. E.; Johansson, M. J.; Pericàs, M. À.; Martín-Matute, B. ChemSusChem 2015, 8, 123.
[25] Kong, S. N.; Malik, A. U.; Qian, X. F.; Shu, M. H.; Xiao, W. D. Chin. J. Org. Chem. 2018, 38, 432(in Chinese). (孔胜男, Abaid Ullah Malik, 钱雪峰, 舒谋海, 肖文德, 有机化学, 2018, 38, 432.)
[26] Tan, L.; Tan, B. Chem. Soc. Rev. 2017, 46, 3322.
[27] Wang, S.; Song, K.; Zhang, C.; Shu, Y.; Li, T.; Tan, B. J. Mater. Chem. A 2017, 5, 1509.
[28] Xu, S.; Song, K.; Li, T.; Tan, B. J. Mater. Chem. A 2015, 3, 1272.
[29] Massaro, M.; Riela, S.; Lazzara, G.; Gruttadauria, M.; Milioto, S.; Noto, R. Appl. Organomet. Chem. 2014, 28, 234.
[30] Wang, S.; Zhang, C.; Shu, Y.; Jiang, S.; Xia, Q.; Chen, L.; Jin, S.; Hussain, I.; Cooper, A. I.; Tan, B. Sci. Adv. 2017, 3.
[31] Huang, Y.; Yang, L.; Huang, M.; Wang, J.; Xu, L.; Li, W.; Zhou, H.; Sun, X.; Xing, H.; Liu, H. Particuology 2015, 22, 128.
[32] Li, B.; Yang, X.; Xia, L.; Majeed, M. I.; Tan, B. Sci. Rep. 2013, 3, 2128.
[33] Li, L.; Cui, C.; Su, W.; Wang, Y.; Wang, R. Nano Res. 2016, 9, 779.
[34] Yang, X.; Song, K.; Tan, L.; Hussain, I.; Li, T.; Tan, B. Macromol. Chem. Phys. 2014, 215, 1257.
[35] Sun, Y.; Zhao, J.; Wang, J.; Tang, N.; Zhao, R.; Zhang, D.; Guan, T.; Li, K. J. Phys. Chem. C 2017, 121, 10000.
[36] Feng, Z.; Wei, W.; Wang, L.; Hong, R. RSC Adv. 2015, 5, 96911.
[37] Ozer, O.; Ince, A.; Karagoz, B.; Bicak, N. Desalination 2013, 309, 141.
[38] Chen, X.; Cheng, Y.; Seo, C. Y.; Schwank, J. W.; McCabe, R. W. Appl. Catal. B 2015, 163, 499.
[39] He, Y.; Liang, L.; Liu, Y.; Feng, J.; Ma, C.; Li, D. J. Catal. 2014, 309, 166.
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