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化学学报
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化学学报 ›› 1965, Vol. 31 ›› Issue (4): 336-337. 上一篇    下一篇

研究简报

2,2-双[4-羟基-3,5-二碘代苯基]丙烷的合成

隋振恩, 張玉珍, 李翠鳳, 王順貞, 楊玲   

  1. 中国科学院华北化学研究所
  • 投稿日期:1964-07-16 发布日期:2013-06-03

SYNTHESIS OF 2,2-BIS[4-HYDROXY-3,5-DⅡODOPHENYL] PROPANE

SUI ZHEN-EN, ZHANG YU-ZHEN, LI CUI-FENG, WANG SHUN-ZHEN, YANG LING   

  1. Hua-Bei Institute of Chemistry, Academia Sinica, Tiensien
  • Received:1964-07-16 Published:2013-06-03

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含氯和溴的2,2-双[4-羟基-3,5-二卤代苯基大]丙烷(卤代双酚-A)已见专利和文献,而相应碘代化合物尚无报导.

The titled compound (tetraiodobisphenol-A) was synthesized by the action of iodine on 2,2-bis[4-hydroxy-phenyl]propane (bisphenol-A) in aqueous ammonium hydroxide solution at room temperature.The tetraiodobisphenol-A is a colourless crystalline substance, melting at 271-272° (decompn.).It reacts with epichlorohydrin to give a deep-brown resin.