Synthesis of derivatives of 2',5'- dithydropyrrolo [3',4':1,2][60] fullerene

Acta Chimica Sinica ›› 1999, Vol. 57 ›› Issue (7): 812-819. Previous Articles Next Articles

Original Articles

2',5'-二氢-1'H-吡咯骈[3',4':1,2][60]富勒烯衍生物的合成

吴世晖;李文玉;张丹维;高翔;李越生;吴厚铭;徐静斐

复旦大学化学系.上海(200433);复旦大学材料科学系.上海(200433);中国科学院上海有机化学研究所.上海(200032);中国科学院生命有机国家重点实验室

发布日期:1999-07-15

Synthesis of derivatives of 2',5'- dithydropyrrolo [3',4':1,2][60] fullerene

Wu Shihui;Li Wenyu;Zhang Danwei;Gao Xiang;Li Yuesheng;Wu Houming;Xu Jingfei

Fudan Univ, Dept Chem.Shanghai(200433);Fudan Univ, Dept of Material Sci.Shanghai(200433);Shanghai Inst Organ Chem., CAS.Shanghai(200032)

Published:1999-07-15

Abstract

[60]Fullerene reacts with imines prepared from substituted benzaldehydes and α-amino acid ester to give isomers of fullerene- fused proline derivatives via 1,3-dipolar cycloaddition. The products were characterized by FT-IR,UV-vis,^1H NMR,^1^3C NMR and TOF-SIMS spectroscopic techniques. The bioactivities of the products were also tested.

Key words: PYRROLIDINE, FULLERENES, GLYCINE, ACETIC ACID P, BENZALDEHYDE P, IMINE, PROTON MAGNETIC RESONANCE SPECTROMETRY, C13 NMR SPECTROMETRY, FOURIER TRANSFORM, INFRARED SPECTROPHOTOMETRY

CLC Number:

O621

Cite this article

Wu Shihui;Li Wenyu;Zhang Danwei;Gao Xiang;Li Yuesheng;Wu Houming;Xu Jingfei. Synthesis of derivatives of 2',5'- dithydropyrrolo [3',4':1,2][60] fullerene[J]. Acta Chimica Sinica, 1999, 57(7): 812-819.

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2',5'-二氢-1'H-吡咯骈[3',4':1,2][60]富勒烯衍生物的合成

Synthesis of derivatives of 2',5'- dithydropyrrolo [3',4':1,2][60] fullerene

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