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Acta Chimica Sinica ›› 1957, Vol. 23 ›› Issue (6): 438-446. Previous Articles     Next Articles

碘杂環化合物的研究Ⅱ.3,6-二-[二甲氨基]-二苯并碘六圜(Ⅲ)鹽的合成及其性質

黄文魁   

  1. 蘭州大学化学系
  • 投稿日期:1957-05-21 发布日期:2013-06-03

STUDIES ON HETEROCYCLIC COMPOUNDS CONTAINING IODINE Ⅱ. THE SYNTHESIS OF 3, 6-DI-[DIMETHYLAMINO]-DIBENZOPYRIODONIUM SAINTS (Ⅲ) AND THEIR PROPERTIES

HWAND WEN-KUET   

  1. Department of Chemistry, Lanchow University, Lanchow
  • Received:1957-05-21 Published:2013-06-03

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Reac6ion between 4,4'-di-〔dimethylamino〕-diphenylmethane(Ⅰ) and iodosyl sulfate (Ⅱ) in concon6rated sulfuric acid solution gave an iodine heterocycle,3,6-di-[dimethylamino]-dibenzopyriodonium iodide dihydriodide(Ⅲa·2HI),m.p.179-181°(decomp.),with a yiold of 77%.