化学学报 ›› 1959, Vol. 25 ›› Issue (6): 420-423. 上一篇    下一篇

研究简报

用气液色谱法分离甲基氯硅烷和鉴定的研究

余仲建1,2, 杨学谨1,2, 粟富经1,2, 谢珍珍1,2, 刘静华1,2   

  1. 1. 中国科学院河北分院元素有机研究所;
    2. 南开大学化学系
  • 投稿日期:1959-07-30 发布日期:2013-06-03

GAS-LIQUID CHROMATOGRAPHIC SEPARATION AND IDENTIFICATION OF METHYLCHLOROSILANES

YU CHUNG-CHIEN1,2, YANG HSÜEH-CHING1,2, SU FU-CHING1,2, HSIEH CHEN-CHEN1,2, LIU CHING-HUA1,2   

  1. Department of Chemistry, Nankai University
  • Received:1959-07-30 Published:2013-06-03

1.二苯甲酮适用于作分离和鉴定甲基氯硅烷的固定相。2.在较低的温度下(52℃)能将甲基三氯硅烷,二甲基二氯硅烷,三甲基(?)氯硅烷和四氯化硅混合物中的各组分完全分开。

Benzophenone has been found to be a suitable fixed phase for gas-liquid chromato-graphy of methylchlorosilanes.Good separation of methyltrichlorosilane, dimethyldichlorusi-lane, trimethylchlorosilane and silicon tetrachloride was obtained at 52℃.