化学学报 ›› 1960, Vol. 26 ›› Issue (2): 108-110. 上一篇    下一篇

研究简报

过滤沉淀法快速分离新钍Ⅰ和新钍Ⅱ

孙亦梁, 朱芝仙, 陆永基   

  1. 北京大学
  • 投稿日期:1959-08-18 发布日期:2013-06-03

SEPARATION OF MsTh-Ⅰ FROM M8Th-Ⅱ BY FILTRATION-PRECIPITATION METHOD

SUN YI-LIANG, CHU ZHI-XIAN, LU YONG-JI   

  1. Piking University
  • Received:1959-08-18 Published:2013-06-03

自新钍中提取新钍Ⅱ已有不少方法.Gmelin[1]综述一九四二年以前的工作.Seaborg,sup>[2]增加了若干新方法.按分离难易和原料有关.制备新钍Ⅱ最好以老的钍盐中分出的新钍作原料,而不以钍矿为原料,因为钍矿往往含镭-226及其子体.近年来用于Ac227和AcX(Ra223)等同位素分离的TTA萃取法和以硝酸为淋洗液的阳离子交换法均可应用于新钍Ⅰ和Ⅱ的分离。

Carrier-free MsTh-Ⅱ can be rapidly separated from its parent MsTh-Ⅰ by filtering its neutral solution through an anion exchanger [OH] column, MsTh-Ⅱ being precipitated on the resin. MsTh-Ⅱ can be eluted from the column with hydrochloric acid. The separation takes about half an hour.