化学学报 ›› 1980, Vol. 38 ›› Issue (1): 50-56. 上一篇    下一篇

论文

用X射线衍射法快速测定聚对次苯基硫醚的结晶度Ⅱ.

陈济舟1, 蒋世承2   

  1. 1. 天津化工研究院;
    2. 河北工学院
  • 投稿日期:1978-01-29 发布日期:2013-06-03

THE RAPID DETERMINATION OF CRYSTALLINITY IN POLY-P-PHENYLENE SULFIDE BY X-RAY DIFFRACTION METHOD Ⅱ.

CHEN JI-ZHOU1, JIANG SHI-CHENG2   

  1. 1. Tianjin Institute of Chemical Engneering;
    2. Hebei college of Technology
  • Received:1978-01-29 Published:2013-06-03

本文报道用X射线衍射测定聚对次苯基硫醚(pps)结晶度的一个快速测定方法:即选择(110)峰和峰的积分面积与对应的非晶散射峰的积分面积代表它们的强度来计算聚对次苯基硫醚的结晶度,利用这个方法测定了聚对次苯基硫醚原粉和在不同温度下热处理后样品的结晶度,最后得到了比较满意的结果。

This investigation describes a method in which the crystallinitp of pps is determined by measuring the heights of (110) and peaks in the X-ray diffraction pattern,and compensated by factors C and A.