化学学报 ›› 1987, Vol. 45 ›› Issue (10): 987-992. 上一篇    下一篇

研究论文

含磷稠环8,9,16,17-四脱氢-6,14-二硫羰基-6,14-三巯基-7,8,15,16-四氮-5,13-二氧-6,14-二磷杂二苯并[a,b]蒽烷吡啶盐及其衍生物的合成和结构

陈其杰;金淑娟;缪方明;王瑾玲   

  1. 南开大学元素有机化学研究所;天津师范大学化学系
  • 发布日期:1987-10-15

Synthesis and structure of fused ring compound containing phosphorus 8,9,16,17-tetradehydro-6,14-=dithiono-6,14-dithiol-7,8,15,16-tetraza-5, 13-dioxa-6,14-diphosphadibenzo(ah)tetradecahydro-anthracene pyridinium and its derivatives

CHEN QIJIE;JIN SHUJUAN;MIAO FANGMING;WANG JINLING   

  • Published:1987-10-15

关键词: 晶体结构测定, 分子结构, X射线衍射分析, 质谱法, 氮杂环化合物, 质子磁共振谱法, 硫代氨基膦酸 P, 氧杂环化合物, 磷杂环化合物, 稠环化合物

The syntheses of the title compound and its eleven derivatives I (R = alkyl, benzyl, allyl, CH2CO2Et) are described. The crystal and mol. structures of the pyridinium compound and its several derivatives were also determine

Key words: CRYSTAL STRUCTURE DETERMINATION, MOLECULAR STRUCTURE, X-RAY DIFFRACTION ANALYSIS, MASS SPECTROGRAPHY, NITROGEN HETEROCYCLICS, PROTON MAGNETIC RESONANCE SPECTROMETRY, PHOSPHONAMIDOTHIOIC ACID P, OXYGEN HETEROCYCLICS, PHOSPHOROUS HETEROCYCLIC COMPOUNDS, FUSED RING COMPOUNDS

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