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化学学报 ›› 1963, Vol. 29 ›› Issue (2): 86-89. 上一篇 下一篇
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周維善
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CHOW WEI-ZAN
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△6-6-甲基螺甾内酯(Ⅷ)可从环氧化合物(Ⅱ)经Grignard试剂一步加入6-甲基及侧链羧基,继用常法氢化、氧化、脱水、脱氢等步骤合成。
△6-6-methyl spirolactone (VⅢ) was synthesized from epoxide (Ⅱ) through the following series of reaction, viz, Grignard synthesis with the introduction of 6-methyl and side chain carboxyl groups simultaneously, followed by catalytic hydrogenation, chromic acid oxidation, dehydration and dehydrogenation.L5
周維善. △6-6-甲基螺甾内酯的合成[J]. 化学学报, 1963, 29(2): 86-89.
CHOW WEI-ZAN. SYNTHESIS OF △6-6-METHYL SPIROLACTONE[J]. Acta Chimica Sinica, 1963, 29(2): 86-89.
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