Studies on synthesis and structure of ethylenebis-(2,2,5,5-tetramethyl-1-aza-2,5-disilacyclopentane)

Acta Chimica Sinica ›› 1987, Vol. 45 ›› Issue (5): 456-460. Previous Articles Next Articles

Original Articles

乙撑双(2,2,5,5-四甲基-1-氮-2,5-二硅环戊烷)的合成及结构

张宝申;周秀中;缪方明;刘小兰

南开大学化学系;天津师范大学化学系

发布日期:1987-05-15

Studies on synthesis and structure of ethylenebis-(2,2,5,5-tetramethyl-1-aza-2,5-disilacyclopentane)

ZHANG BAOSHEN;ZHOU XIUZHONG;MIAO FANGMING;LIU XIAOLAN

Published:1987-05-15

Abstract

Heating 2,2,5,5-tetramethyl-1-aza-2,5-disilacyclopentane or bis(diethylaminodimethylsilyl)ethane with ethylenediamine and a small amount of (NH4)2SO4 gave the title compound (I) in 71 and 62% yield resp. The crystal structure of I was determine

Key words: CRYSTAL STRUCTURE DETERMINATION, NITROGEN HETEROCYCLICS, FIVE MEMBER RING HETEROCYCLIC COMPOUNDS, SILICON HETEROCYCLICS COMPOUNDS, SILAZANE, ETHANEDIAMINE P

CLC Number:

O627

Cite this article

ZHANG BAOSHEN;ZHOU XIUZHONG;MIAO FANGMING;LIU XIAOLAN. Studies on synthesis and structure of ethylenebis-(2,2,5,5-tetramethyl-1-aza-2,5-disilacyclopentane)[J]. Acta Chimica Sinica, 1987, 45(5): 456-460.

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乙撑双(2,2,5,5-四甲基-1-氮-2,5-二硅环戊烷)的合成及结构

Studies on synthesis and structure of ethylenebis-(2,2,5,5-tetramethyl-1-aza-2,5-disilacyclopentane)

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