Acta Chimica Sinica ›› 1996, Vol. 54 ›› Issue (10): 1023-1029. Previous Articles     Next Articles

Original Articles

1-芳基-5-苯并三唑基-1-戊烯的合成及其位置异构体的GC-MS研究

丁明武;石德清;肖文精;黄文芳;吴田捷   

  1. 华中师范大学有机合成研究所;华中师范大学分析测试中心
  • 发布日期:1996-10-15

Synthesis of 1-aryl-5-benzotriazolyl-1-pentenes and GC-MS studies on their tautomers

DING MINGWU;SHI DEQING;XIAO WENJING;HUANG WENFANG;Wu Tianjie   

  • Published:1996-10-15

1-Aryl-5-benzotriazolyl-1-pentenes (3 and 3') can be prepared via two synthetic routes. The compositions of their four isomers were analyzed by GC-MS. The 1-N and 2-N tautomers can be distinguished conveniently from whether the ion peaks of [M-29]^+^· and [M-57]^+^· are rich or not.

Key words: WITTIG REACTION, BENZOTRIAZOLE P, CHROMATOGRAPHY-MASS SPECTROGRAPHY

CLC Number: