Polyaniline function materials doped with H3+nPMo12- nVnO40(n=0,1) have been prepared by a new method where in the heteropolyacid acts as both proton acid and oxidizer without using other proton acid and oxidizer during the synthesis reaction. These materials were characterized by IR, Vis-NIR, 31^P NMR, XRD. The materials exhibit conductivity and fluorescence property.

Key words: POLYANILINE, ELECTRICAL CONDUCTIVITY, FLUORESCENCE MATERIALS, INORGANIC MATERIALS, SYNTHESIS METHODS, HETEROPOLYACID, DOPE EFFECT