Effect of Carrying Gas on Preparation of Carbon Nanotubes and Nanofibers by an Injection Chemical Vapor Deposition Method

Acta Chimica Sinica ›› 2004, Vol. 62 ›› Issue (22): 2253-2258. Previous Articles Next Articles

载气对注入CVD法制备碳纳米管和碳纳米纤维的影响

张兵, 郭燕川, 陈丽娟, 彭必先

中国科学院理化技术研究所, 北京, 100101

投稿日期:2004-03-01 修回日期:2004-07-12 发布日期:2014-02-17
通讯作者: 彭必先,E-mail:pengbx@ipc.ac.cn E-mail:pengbx@ipc.ac.cn

Effect of Carrying Gas on Preparation of Carbon Nanotubes and Nanofibers by an Injection Chemical Vapor Deposition Method

ZHANG Bing, GUO Yan-Chuan, CHEN Li-Juan, PENG Bi-Xian

Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100101

Received:2004-03-01 Revised:2004-07-12 Published:2014-02-17

Abstract

Aligned multi-walled carbon nanotubes and nanofiber films were grown in quartz tube reactor by an injection chemical vapor deposition method. Various carbon materials were produced with different carrying gas in the same system. Scanning electron microscope images, transmission electron microscope images and Raman spectrum reveal that carbon nanofibers synthesized in inert gases have highly crystalline properties and iron particles were circled with nanofiber wall, and carbon nanotubes with hollow cavity were prepared in hydrogen gas. The distribution of diameters was controlled by changing the ratio of hydrogen to inert gases.

Key words: carbon nanotube, carbon nanofiber, injection CVD, carrying gas, morphology

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ZHANG Bing, GUO Yan-Chuan, CHEN Li-Juan, PENG Bi-Xian. Effect of Carrying Gas on Preparation of Carbon Nanotubes and Nanofibers by an Injection Chemical Vapor Deposition Method[J]. Acta Chimica Sinica, 2004, 62(22): 2253-2258.

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载气对注入CVD法制备碳纳米管和碳纳米纤维的影响

Effect of Carrying Gas on Preparation of Carbon Nanotubes and Nanofibers by an Injection Chemical Vapor Deposition Method

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