Acta Chimica Sinica ›› 2010, Vol. 68 ›› Issue (06): 571-575. Previous Articles     Next Articles

Full Papers

静电纺丝法制备聚乳酸/纳米磷酸钙复合纳米纤维及其表征

李从举*,1,2,黄丽1,肖斌1,冯苹1   

  1. (1北京服装学院材料科学与工程学院 北京 100029)
    (2北京市服装材料研究开发与评价重点实验室 北京 100029)
  • 投稿日期:2009-07-07 修回日期:2009-09-09 发布日期:2010-03-28
  • 通讯作者: 李从举 E-mail:congjuli@iccas.ac.cn
  • 基金资助:

    国家自然科学基金,国家863计划,PHR项目

Preparation and Characterization of Poly(lactic acid)/nano-calcium Phosphate Composite Nanofibers by Electrospinning

Li Congju*,1,2 Huang Li1 Xiao Bin1 Feng Ping1   

  1. (1 School of Material Science and Engineering, Beijing Institute of Fashion Technology, Beijing 100029)
    (2 Beijing Key Laboratory of Clothing Materials R&D and Assessment, Beijing 100029)
  • Received:2009-07-07 Revised:2009-09-09 Published:2010-03-28
  • Contact: LI Cong-Ju E-mail:congjuli@iccas.ac.cn

Nano-calcium phosphate (NCP) was firstly synthesized, and then characterized by scanning electronic microscopy (SEM) and X-ray diffraction (XRD). Subsequently, PLA/NCP composite nanofibers were obtained by electrospinning, and characterized by TEM, SEM, XRD and uniaxial tensile test. With TEM and XRD results, it was proved that NCP had been successfully incorporated into PLA fibers. As SEM images showed, there was no negative impact on the morphology of the composite fibers when NCP was at low concentrations, however, the morphology would be bad when the concentration was increased to higher than 7%. Then, tensile curves indicated that tensile strength increased with increasing NCP concentration, but decreased when the concentration was higher than 7%.

Key words: electrospinning, nano-calcium phosphate, poly(lactic acid), composite fiber, mechanical strength