Hydrothermal Synthesis and Property Comparation of YF3:Eu3＋Luminescent Nanomaterials with Various Morphology

Acta Chimica Sinica ›› 2010, Vol. 68 ›› Issue (13): 1298-1302. Previous Articles Next Articles

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多种形貌YF₃:Eu^3＋纳米发光材料的水热合成与性能比较

刘桂霞*，张颂，董相廷，王进贤

(长春理工大学化学与环境工程学院长春 130022)

投稿日期:2009-10-23 修回日期:2010-01-21 发布日期:2010-03-04
通讯作者: 刘桂霞 E-mail:liuguixia22@yahoo.com.cn
基金资助:
吉林省科技发展计划资助项目（20090528）

Hydrothermal Synthesis and Property Comparation of YF₃:Eu^3＋Luminescent Nanomaterials with Various Morphology

LIU Gui-Xia, ZHANG Song, DONG Xiang-Ting, WANG Jin-Xian

(School of Chemistry and Environmental Engineering, Changchun University of Science and Technology, Changchun 130022)

Received:2009-10-23 Revised:2010-01-21 Published:2010-03-04

Abstract

Bouquet-shaped, spindle, nanobundle and truncated octahedral YF₃:Eu^3＋nanomaterials were prepared using surfactant-assisted hydrothermal method, the properties and structure were characterized. XRD pattern showed that the samples are all orthogonal phase YF₃ with good crystallization. FESEM and TEM images indicated that the samples with different morphologies are obtained by different surfactants. SEAD photoes showed that the samples are polycrystalline and single crystal, EDX pattern showed that the samples are composed by F, Y and Eu elements. Photoluminescence spectra showed that the strongest emission peak of YF₃:Eu^3＋ nanocrystals is near 591 nm, corresponding to ⁵D₀-⁷F₁ magnetic dipole transition of Eu^3＋, which indicated that Eu^3＋ is sited in C₂-symmetric site of Y^3＋ lattice point in YF₃ host, and it is noted that the emission intensities are different from samples with different morphologies.

Key words: YF₃, morphology, hydrothermal synthesis, luminescent materials

Cite this article

LIU Gui-Xia, ZHANG Song, DONG Xiang-Ting, WANG Jin-Xian. Hydrothermal Synthesis and Property Comparation of YF₃:Eu^3＋Luminescent Nanomaterials with Various Morphology[J]. Acta Chimica Sinica, 2010, 68(13): 1298-1302.

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多种形貌YF₃:Eu^3＋纳米发光材料的水热合成与性能比较

Hydrothermal Synthesis and Property Comparation of YF₃:Eu^3＋Luminescent Nanomaterials with Various Morphology

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多种形貌YF3:Eu3＋纳米发光材料的水热合成与性能比较