The syntheses characterization and crystal structure of rare earth complexes with L-proline

Acta Chimica Sinica ›› 1993, Vol. 51 ›› Issue (3): 257-264. Previous Articles Next Articles

Original Articles

稀土与L-脯氨酸配合物的合成、表征及晶体结构

王增林;牛春吉;胡宁海;倪嘉缵

中国科学院长春应用化学研究所;中国科学院稀土化学与物理开放实验室

发布日期:1993-03-15

The syntheses characterization and crystal structure of rare earth complexes with L-proline

WANG ZENGLIN;NIU CHUNJI;HU NINGHAI;NI JIAZUAN

Published:1993-03-15

Abstract

ML3(H2O)2(ClO4)3 (M = Pr, Nd, Er; HL = L-proline) and Pr2L6(H2O)4(ClO4)6 (I) were prepared from the metal perchlorates and the amino acid. Crystal data: I; monoclinic, space group P21, a 0.9879(3), b 2.1883(4), c 1.3393(2) nm, b 91.23(2)? Z = 2, R = 0.035. IR and thermal decomposition data are given for the complexes. L is bridging in I and H2O is coordinated.

Key words: INFRARED SPECTROPHOTOMETRY, ELEMENTAL ANALYSIS, CRYSTAL STRUCTURE, PROLINE, RARE EARTH METAL COMPLEX, PERCHLORATE, PRASEODYMIUM COMPLEX, NEODYMIUM COMPLEX, FOUR-CIRCLE DIFFRACTOMETER, ERBIUM COMPLEX

CLC Number:

O611.662

Cite this article

WANG ZENGLIN;NIU CHUNJI;HU NINGHAI;NI JIAZUAN. The syntheses characterization and crystal structure of rare earth complexes with L-proline[J]. Acta Chimica Sinica, 1993, 51(3): 257-264.

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稀土与L-脯氨酸配合物的合成、表征及晶体结构

The syntheses characterization and crystal structure of rare earth complexes with L-proline

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