Hydrothermal Synthesis of Cubic Boron Nitride Crystals

Acta Chimica Sinica ›› 2005, Vol. 63 ›› Issue (10): 909-912. Previous Articles Next Articles

Original Articles

水热法合成立方氮化硼微晶

于美燕*¹，崔得良²，李凯²，尹衍升¹，初蕾¹

(¹中国海洋大学材料科学与工程研究院青岛 266003)
(²山东大学晶体材料研究所济南 250100)

投稿日期:2004-09-13 修回日期:2005-01-24 发布日期:2010-12-10
通讯作者: 于美燕

Hydrothermal Synthesis of Cubic Boron Nitride Crystals

YU Mei-Yan*¹, CUI De-Liang², LI Kai², YIN Yan-Sheng¹, CHU Lei¹

(¹ Institute of Material Science and Engineering, Ocean University of China, Qingdao 266003)
(² State Key Laboratory of Crystal Materials, Shandong University, Jinan 250100)

Received:2004-09-13 Revised:2005-01-24 Published:2010-12-10
Contact: YU Mei-Yan

Abstract

Cubic boron nitride crystals have been successfully synthesized in water solvent at low temperature and low pressure by reaction-coupling effect. The experimental results of X-ray diffraction and Fourier transformation infrared spectroscopy confirmed the phases of product. Furthermore, transmission electron microscopy and selective area electron diffraction indicated the morphology and surface properties of boron nitride. High-resolution transmission electron microscope and X-ray photoelectron spectroscopy measurements proved the existence of cubic boron nitride.

Key words: hydrothermal synthesis, cubic boron nitride, hydrazine hydrate

Cite this article

YU Mei-Yan*, CUI De-Liang², LI Kai², YIN Yan-Sheng, CHU Lei. Hydrothermal Synthesis of Cubic Boron Nitride Crystals[J]. Acta Chimica Sinica, 2005, 63(10): 909-912.

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水热法合成立方氮化硼微晶

Hydrothermal Synthesis of Cubic Boron Nitride Crystals

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