Preparation and Characterization of A Soluble Conducting Polyaniline

Acta Chimica Sinica ›› 2006, Vol. 64 ›› Issue (21): 2210-2214. Previous Articles

Original Articles

一种水中可溶性导电聚苯胺的制备与表征

原玲¹,2, 隋春红¹, 尹荣¹, 龚剑*^,1, 瞿伦玉¹

(¹东北师范大学多酸科学教育部重点实验室长春 130024)
(²内蒙古兴安职业技术学院化学系乌兰浩特 137400)

投稿日期:2005-12-01 修回日期:2006-03-29 发布日期:2006-11-14
通讯作者: 龚剑

Preparation and Characterization of A Soluble Conducting Polyaniline

YUAN Ling¹,2; SUI Chun-Hong¹; YIN Rong¹; GONG Jian*^,1; QU Lun-Yu¹

(¹Key Laboratory of Polyoxometalates Science of Ministry of Education, Northeast Normal University, Changchun 130024)
(²Department of Chemistry, Xingan Occupation Technic College, Wulanhaote 137400)

Received:2005-12-01 Revised:2006-03-29 Published:2006-11-14
Contact: GONG Jian

Abstract

Conducting polyaniline (PANI) doped with H₄SiW₁₂O₄₀ was obtained in the polyglycol (PEG) aqueous solution and PEG ethanol solution, respectively. The PANI was characterized by IR, XRD patterns and UV-Vis spectra. The conductivity of the PANI was measured by the four-probe method. The effect of the ratio of heteropoly acid (HPA), oxidant and aniline, and the temperature of the reaction system on the final yield, conductivity, and solubility of the PANI was investigated, respectively. The results showed that the performance of PANI synthesized in ethanol was better than that in water. The highest conductivity of the PANI prepared in ethanol was 1.87 S/cm. The soluble ratio of the PANI was 53%.

Key words: polyaniline, doping, conductivity, solubility

Cite this article

YUAN Ling^1,2; SUI Chun-Hong; YIN Rong; GONG Jian*^,1; QU Lun-Yu. Preparation and Characterization of A Soluble Conducting Polyaniline[J]. Acta Chimica Sinica, 2006, 64(21): 2210-2214.

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一种水中可溶性导电聚苯胺的制备与表征

Preparation and Characterization of A Soluble Conducting Polyaniline

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