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Acta Chimica Sinica ›› 1965, Vol. 31 ›› Issue (6): 531-535. Previous Articles     Next Articles

二氟一氯甲烷高温溴化产物的气体色谱分析

王永祿1, 郭心正2, 王寿松2, 林永达1   

  1. 1. 中国科学院有机化学研究所;
    2. 浙江化工研究所
  • 投稿日期:1964-10-15 发布日期:2013-06-03

A GAS CHROMATOGRAPHIC ANALYSIS OF HIGH TEMPERATURE BROMINATION PRODUCTS OF DIFLUOROCHLOROMETHANE

WANG YUNG-LUH1, KUO SIN-TSENG2, WANG SHOU-SUNG2, LIN YUNG-DA1   

  1. Institute of Organic Chemistry, Academia Sinica
  • Received:1964-10-15 Published:2013-06-03

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Gas chromatographic analysis of high temperature brommation products of ditluoro chloromethane on a column packed with Liu-Ho firebrick coated with carbowax-400 and dinonyl phthalate(100:5:20, by weight) gave a chromatogram containing twenty peaks, twelve of which were identified as CF2CIBr, CF2Br2, CHF2Br, CF2CI2, CF2BrCF2Br,CF3CFBrCF2Br, CHF2CI, CFCl3, CHFCl2, CF2=CF2, CF3CF=CF2, and CF2·CF2·CF2·CF2.