Research Progress of Microfluidic Technique in Synthesis of Micro/Nano Materials

doi:10.6023/A21030086

Acta Chimica Sinica ›› 2021, Vol. 79 ›› Issue (7): 809-819.DOI: 10.6023/A21030086 Previous Articles Next Articles

Review

微流控技术在微/纳米材料合成中的研究进展

卢佳敏^a, 王慧峰^a^,^c, 潘建章^a^,^b^,^c, 方群^a^,^b^,^c^,^*()

a 浙江大学化学系微分析系统研究所杭州 310058
b 浙江大学浙江省激发态材料合成与应用重点实验室杭州 310027
c 浙江大学杭州国际科创中心杭州 311200

投稿日期:2021-03-09 发布日期:2021-05-17
通讯作者: 方群

作者简介:

卢佳敏, 浙江大学化学系博士研究生. 2019年于厦门大学获得学士学位, 2019年起在方群教授的指导下于浙江大学攻读博士学位, 目前研究方向主要包括微流控分析、流动化学与材料合成.

王慧峰, 浙江大学杭州国际科创中心博士后研究员. 2020年在浙江大学获得分析化学方向理学博士学位. 目前研究方向主要包括微流控分析、流动化学与单细胞分析.

潘建章, 副研究员, 硕士生导师, 致力于微流控分析仪器的微型化、自动化、智能化研究工作. 成功研制掌上激光诱导荧光-毛细管电泳生化分析仪、手持超微量液芯波导光度计、面向航空航天应用的高速毛细管电泳仪、PET显像剂全自动合成仪等微型化自动化微流控仪器. 已发表SCI论文20余篇, 获授权国家发明专利7项, 主持和参与包括国家自然科学基金面上项目、科学仪器研制专项、重大科研仪器研制项目等10余项.

方群, 浙江大学求是特聘教授, 博士生导师, 化学系微分析系统研究所所长, 国家杰出青年基金获得者. 1998年在沈阳药科大学获得药物分析学博士学位. 自1998年开始从事微流控分析的研究工作. 目前研究方向包括微流控液滴分析, 微流控毛细管电泳、液相色谱和质谱分析, 微型化分析系统研制, 以及微流控系统在单细胞分析、微量生化分析、药物筛选和现场分析中的应用. 发表研究论文130余篇. 在微流控分析领域申请国家发明专利40项, 其中26项获得授权. 曾主持承担国家基金委重大项目课题、国家杰出青年基金、国家基金重点项目、科学仪器研制专项和面上项目等.

基金资助:
国家自然科学基金(21827806); 国家自然科学基金(21974122)

Research Progress of Microfluidic Technique in Synthesis of Micro/Nano Materials

Jia-Min Lu^a, Hui-Feng Wang^a^,^c, Jian-Zhang Pan^a^,^b^,^c, Qun Fang^a^,^b^,^c()

a Institute of Microanalytical Systems, Department of Chemistry, Zhejiang University, Hangzhou 310058, China
b Key Laboratory of Excited-State Materials of Zhejiang Province, Zhejiang University, Hangzhou 310027, China
c Hangzhou Innovation Center, Zhejiang University, Hangzhou 311200, China

Received:2021-03-09 Published:2021-05-17
Contact: Qun Fang
Supported by:
National Natural Science Foundation of China(21827806); National Natural Science Foundation of China(21974122)

Micro/nano materials have unique properties that are different from macro materials because of their small scale, and these materials have diverse applications in many fields. In recent years, with the unique advantages of low consumption, high efficiency, high throughput, miniaturization, integration and automation, microfluidic technique has aroused widespread concerns in the synthesis field of micro/nano materials. In this review, the commonly used microreactors are classified from two perspectives of structural form and reaction method, and the application of microfluidic technique in the synthesis of micro/nano materials including inorganic materials, organic materials and composite materials are introduced. In addition, the main development trends in the future are prospected in this review. Microfluidic technique has provided new ideas and methods for the synthesis of micro/nano materials, which has rich possibilities and great potentials in both industrial production and academic research.

Key words: microfluidic technique, flow chemistry, micro/nano material, material synthesis, microreactor

Cite this article

Jia-Min Lu, Hui-Feng Wang, Jian-Zhang Pan, Qun Fang. Research Progress of Microfluidic Technique in Synthesis of Micro/Nano Materials[J]. Acta Chimica Sinica, 2021, 79(7): 809-819.

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Fig. & Tab. 7

Figure 1. Schematic diagram of a typical micro-conduit based (a) microreactor and a microchip-based (b) microreactor[56,58]

Figure 2. Schematic diagram of a typical batch microreactor[66] (a) and a continuous-flow microreactor[59] (b). (b1) Continuous flow mode; (b2) segmented flow mode; (b3) droplet flow mode

Figure 3. (a) Synthesis of CsPbX3 quantum dots based on droplet microreactors[100]; (b) multi-stage microfluidic platform that can connect up to six chip reactors in series[101]

Figure 4. Shorten the life of the intermediate through the design of the channel. (a) Shorten the residence time of the intermediate[108]; (b) mixed area with 3D serpentine channel[112]

Figure 5. (a, b) Aqueous Janus microparticles formed by consolidation of toluene emulsion drops of PS and PLA dispersed in an aqueous polyethylene oxide-polypropylene oxide triblock copolymer solution[136]

Figure 6. (a) Schematic illustration of MOFs synthesized by droplet microfluidic system[145]; (b) preparation of MOFs with uniform graded pores by microfluidic system[148]

Figure 7. (a) Schematic of a microreactor integrated with an online NIR fluorescence detection system[149]; (b) schematic workflow for automatic feedback optimization and kinetic data extraction using a microfluidic system[153]

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微流控技术在微/纳米材料合成中的研究进展

Research Progress of Microfluidic Technique in Synthesis of Micro/Nano Materials

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